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Analytical Letters Volume 34, 2001 - Issue 8
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Original Articles

DETERMINATION OF HYDRAZINE BY FLOW INJECTION WITH CHEMILUMINESCENCE

Jiagen Lv Department of Chemistry, Shaanxi Normal University, Xi'an, 710062, P. R. China
,
Yuming Huang Department of Chemistry, Southwest Normal University, Beibei, Chongqing, 400715, P. R. China
&
Zhujun Zhang Department of Chemistry, Southwest Normal University, Beibei, Chongqing, 400715, P. R. China
Pages 1323-1330 | Received 20 Sep 2000, Accepted 12 Feb 2001, Published online: 02 Feb 2007
 
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Abstract

The oxidation of hydrazine by potassium hexacyanoferrate(III) in alkaline luminol solution leads to chemiluminescence. This can be used to determine individual hydrazines using flow injection system. Calibration data are reported for 2,4-dinitrophenylhydrazine, isoniazid, N-acetylphenylhydrazine, and hydrazine sulfate. The system has been successfully applied to the determination of isoniazid in pharmaceuticals and hydrazine in air, respectively.

ACKNOWLEDGMENTS

This work is supported by the Natural Science Foundations of China and the Natural Science Foundations of Chongqing.

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