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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 20
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Original Articles

HYPERVALENT IODINE IN SYNTHESIS. 66. ONE POT PREPARATION OF β-KETO SULFONES BY REACTION OF KETONES, [HYDROXY(TOSYLOXY) IODO] BENZENE, AND SODIUM SULFINATES

Yuan-Yuan Xie Department of Chemistry, Zhejiang University (Xi-Xi campus), Hangzhou, 310028, P. R. China
&
Zhen-Chu Chen Department of Chemistry, Zhejiang University (Xi-Xi campus), Hangzhou, 310028, P. R. China
Pages 3145-3149 | Received 02 Jan 2001, Published online: 16 Aug 2006
 
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Abstract

One pot reactions of ketones, [hydroxy(tosyloxy)iodo] benzene and sodium sulfinates lead to the formation of the corresponding β-keto sulfones under mild conditions and in good yield.

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