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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 2
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Original Articles

REDUCTION OF N-2-SUBSTITUTED BENZIMIDAZOYL IMIDATES

R. Abderrahim Faculté des Sciences de Tunis, Laboratoire d'Electrochimie, Campus Universitaire, 1060 Le Belvedere, Tunis, Tunisia
,
H. Medini Faculté des Sciences de Tunis, Laboratoire d'Electrochimie, Campus Universitaire, 1060 Le Belvedere, Tunis, Tunisia
,
R. Kossai Faculté des Sciences de Tunis, Laboratoire d'Electrochimie, Campus Universitaire, 1060 Le Belvedere, Tunis, Tunisia
&
K. Boujlel Faculté des Sciences de Tunis, Laboratoire d'Electrochimie, Campus Universitaire, 1060 Le Belvedere, Tunis, Tunisia
Pages 241-248 | Received 17 Jun 2000, Published online: 16 Aug 2006
 
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ABSTRACT>

Cathodic reduction of several iminoesters ( 1 ) and ( 2 ) has been investigated by cyclic voltammetry and controlled potential electrolysis at mercury electrode in aprotic DMF, leading to the formation of two reduction steps. The appropriate choice of the nature of R2 groups allowed the reductive cyclisation when R2 is an ethoxy (or alkoxy) group.

ACKNOWLEDGMENTS

The authors thank SERST (Lab-CH02) for financial support and assistance.

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