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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 18
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Original Articles

EFFICIENT AND CONVENIENT SYNTHESIS OF 3,4,5-TRIMETHOXYBENZALDEHYDE FROM p-CRESOL

Ya-Fei Ji School of Chemical Engineering, China University of Mining and Technology, Xuzhou, Jiangsu, 221008, P.R. ChinaCorrespondence[email protected]
,
Zhi-Min Zong School of Chemical Engineering, China University of Mining and Technology, Xuzhou, Jiangsu, 221008, P.R. China
&
Xian-Yong Wei School of Chemical Engineering, China University of Mining and Technology, Xuzhou, Jiangsu, 221008, P.R. ChinaCorrespondence[email protected]
Pages 2809-2814 | Received 31 Jul 2001, Published online: 18 Oct 2011
 
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ABSTRACT

With p-cresol as starting material, 3,4,5-trimethoxybenzaldehyde was synthesized in an overall yield of 67.4% via bromination, hydrolysis, methoxylation and methylation.

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