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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 20
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Original Articles

PREPARATION OF 1-INDANONES WITH CONVENTIONAL HEATING VERSUS MICROWAVES

Erick S. da Camara e Silva Departamento de Engenharia Química, Instituto Militar de Engenharia, Rio de Janeiro, 22290-270, Brazil
,
J. D. Figueroa-Villar Departamento de Engenharia Química, Instituto Militar de Engenharia, Rio de Janeiro, 22290-270, Brazil
&
Alcino Palermo de Aguiar Departamento de Engenharia Química, Instituto Militar de Engenharia, Rio de Janeiro, 22290-270, BrazilCorrespondence[email protected]
Pages 3193-3198 | Received 24 Oct 2001, Published online: 16 Aug 2006
 
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ABSTRACT

The acylation reactions of p-methylphenol with crotonic and 2-octenoic acids was carried out with the employment of conventional heating and irradiation by microwaves. The use of microwaves led to a significant reduction in the time of reaction from several hours to 2 min and 30–60% yield

ACKNOWLEDGMENT

The authors thanks Marcus Henrique (Polo Xistoquímico IQ/UFRJ) and Dr. Rosane San Gil and Cristiane Parpinelli (Lab. NMR of IQ/UFRJ) for some of the spectral analyses.

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