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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 23
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Original Articles

OXIDATION OF ALKYLCYANOHYDRAZINES TO AZO-BIS NITRILES USING OXONE®–POTASSIUM BROMIDE IN AQUEOUS MEDIUM

B. V. Tamhankar Department of Chemistry, Shivaji University, Kolhapur, 416 004, India
,
Uday V. Desai Department of Chemistry, Shivaji University, Kolhapur, 416 004, IndiaCorrespondence[email protected]
,
R. B. Mane Department of Chemistry, Shivaji University, Kolhapur, 416 004, India
,
P. P. Kulkarni Department of Chemistry, Shivaji University, Kolhapur, 416 004, India
&
P. P. Wadgaonkar Polymer Division, National Chemical Laboratory, Pune, 411 008, India
Pages 3643-3646 | Received 03 Jul 2001, Published online: 16 Aug 2006
 
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ABSTRACT

Azo-bis nitriles were prepared in good yields and high purity by oxidation of corresponding 1,2-bis-dialkylcyano hydrazines using oxone-potassium bromide in aqueous medium.

ACKNOWLEDGMENTS

BVT thanks UGC, New Delhi for the award of fellowship under Faculty Improvement programme.

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