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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 3
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Original Articles

A Convenient Synthesis of Conjugated ω-Arylpolyenals via Wittig Reaction with (1,3-Dioxan-2-yl-methyl)triphenylphosphonium Bromide/Sodium Hydride

Damian Plażuk Department of Organic Chemistry, University of Łódź, Łódź, Narutowicza 68, Poland
,
Izabela Janowska Department of Organic Chemistry, University of Łódź, Łódź, Narutowicza 68, Poland
,
Arkadiusz Kłys Department of Organic Chemistry, University of Łódź, Łódź, Narutowicza 68, Poland
,
Asia Hameed Department of Organic Chemistry, University of Łódź, Łódź, Narutowicza 68, Poland
&
Janusz Zakrzewski Department of Organic Chemistry, University of Łódź, Łódź, Narutowicza 68, PolandCorrespondence[email protected]
Pages 381-385 | Received 07 Jan 2002, Published online: 17 Aug 2006
 
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Abstract

Commercially available reagent, (1,3-dioxan-2-yl-methyl)triphenylphosphonium bromide, sodium hydride and a catalytic amount of 18-crown-6 has proven efficient system for vinylic extension of ο-arylpolyenals.

Acknowledgment

The financial support by the Polish State Committee for Scientific Research (Grant 3T09 A 027 16) is gratefully acknowledged.

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