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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 14
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Original Articles

Chemo-enzymatic Preparations of (R)- and (S)-3-Iodocyclohex-2-en-1-yl Acetate

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Pages 2487-2496 | Received 22 May 2002, Published online: 20 Aug 2006
 

Abstract

Kinetic resolutions by lipase-catalyzed transesterification with 3-iodocyclohex-2-en-1-ol or 3-iodocyclohex-2-en-1-yl acetate followed by inversion of the chirality of the optically active alcohol without separation from the acetate have allowed the preparation of (R)- and (S)-3-iodocyclohex-2-en-1-yl acetate with more than 70% yield and more than 85% ee.

Acknowledgment

We are grateful to Novo Nordisk A/S (Denmark) for a gift of Novozym®.

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