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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 6
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Original Articles

Mono‐nitration of Coumarins by Nitric Oxide

Liandi Lei State Key Laboratory of Applied Organic Chemistry, Lanzhou University, Lanzhou, 730000, China
,
Desuo Yang State Key Laboratory of Applied Organic Chemistry, Lanzhou University, Lanzhou, 730000, China
,
Zhongquan Liu State Key Laboratory of Applied Organic Chemistry, Lanzhou University, Lanzhou, 730000, China
&
Longmin Wu State Key Laboratory of Applied Organic Chemistry, Lanzhou University, Lanzhou, 730000, ChinaCorrespondence[email protected]
Pages 985-992 | Received 25 Jul 2003, Published online: 21 Aug 2006
 
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Abstract

A novel methodology for the efficient and selective nitration of coumarins has been developed. The reaction of coumarins containing a hydroxy group with nitric oxide in CH2Cl2 or CH3CN gave aromatic mono‐ and regio‐specific‐nitrated coumarins in various yields.

Acknowledgment

The authors thank The Natural Science Foundation of China for the financial support (The grant No 20272022).

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