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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 6
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Original Articles

An Efficient Method for Synthesis of 4‐(Phosphonomethyl)benzene Derivatives Under Solvent‐Free Conditions

Ting Yang Key Laboratory of Bioorganic Phosphorus Chemistry, Ministry of Education, Department of Chemistry, School of Life Sciences and Engineering, Tsinghua University, Beijing, 100084, P.R. China
,
Changxue Lin Key Laboratory of Bioorganic Phosphorus Chemistry, Ministry of Education, Department of Chemistry, School of Life Sciences and Engineering, Tsinghua University, Beijing, 100084, P.R. China
,
Hua Fu Key Laboratory of Bioorganic Phosphorus Chemistry, Ministry of Education, Department of Chemistry, School of Life Sciences and Engineering, Tsinghua University, Beijing, 100084, P.R. ChinaCorrespondence[email protected]
,
Yuyang Jiang Key Laboratory of Bioorganic Phosphorus Chemistry, Ministry of Education, Department of Chemistry, School of Life Sciences and Engineering, Tsinghua University, Beijing, 100084, P.R. China
&
Yufen Zhao Key Laboratory of Bioorganic Phosphorus Chemistry, Ministry of Education, Department of Chemistry, School of Life Sciences and Engineering, Tsinghua University, Beijing, 100084, P.R. China
Pages 1017-1022 | Received 03 Jul 2003, Published online: 21 Aug 2006
 
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Abstract

A simple, efficient and general method has been developed for synthesis of 4‐(phosphonomethyl)benzene derivatives through one‐pot reaction of phosphoric acid, 4‐substitute benzyl chlorides and hexamethyldisilazane under solvent‐free conditions and the following hydrolysis in 2M NH4OH.

Acknowledgments

The authors would like to thank the financial support from the Excellent Dissertation Foundation by the Chinese Ministry of Education (No. 200222).

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