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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 23
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Original Articles

One‐Pot Synthesis of Ene‐Lactams via N‐Debenzylation of Keto‐Containing N‐2,4‐Dimethoxylbenzylamides

Wai Ming Kan Department of Pharmacology, National Cheng Kung University, Tainan, Taiwan, R.O.C.
,
Ching‐Lung Cheng Department of Applied Chemistry, National Chiayi University, Chiayi, Taiwan, R.O.C.
&
Ching‐Yuh Chern Department of Applied Chemistry, National Chiayi University, Chiayi, Taiwan, R.O.C.Correspondence[email protected]
Pages 4257-4264 | Received 10 May 2004, Published online: 10 Jan 2011
 
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Abstract

A general method of ene‐lactam preparation is described. Ene‐lactams can be prepared efficiently from keto‐containing N‐2,4‐dimethoxylbenzylamides in good to excellent yields. This method is applicable for the preparation of substituted δ‐, γ‐, and ϵ‐ene‐lactams and bicyclic ene‐lactams.

Acknowledgment

This work was supported by the National Science Council, Taiwan, R.O.C. grants NSC92‐2113‐M415‐004.

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