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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 35, 2005 - Issue 2
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Original Articles

A Mild, Efficient, and Green Procedure for Michael Addition of Active Methylene Compounds to Chalcones Under Microwave Irradiation

Satya Paul Department of Chemistry, University of Jammu, Jammu, 180 006, IndiaCorrespondence[email protected]
,
Monika Gupta Department of Chemistry, University of Jammu, Jammu, 180 006, India
,
Parvinder Pal Singh Department of Chemistry, University of Jammu, Jammu, 180 006, India
,
Rajive Gupta Department of Chemistry, University of Jammu, Jammu, 180 006, India
&
André Loupy Laboratoire des Réactions Sélectives sur Supports, CNRS UMR 8615, ICMMO, Université Paris‐Sud, Orsay Cedex, France
Pages 325-332 | Received 10 Jun 2004, Published online: 28 Jul 2007
 
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Abstract

A simple, rapid, and highly efficient method has been developed for the Michael addition of active methylene compounds to chalcones using potassium carbonate and water under microwave irradiation. The method is totally exempt of organic solvents, and pure products were obtained in good to excellent yields. This method can be used for the parallel synthesis and further scale‐up to 50 mmol of substrate.

Acknowledgment

One of the authors (MG) is thankful to Council of Scientific and Industrial Research (CSIR), New Delhi, for awarding Junior Research Fellowship (JRF).

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