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Research Papers

Secondary hardened bainite

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Pages 1014-1023 | Received 01 Oct 2013, Accepted 04 Mar 2014, Published online: 14 Apr 2014

Figures & data

Table 1. Compositions of three hot rolled strips/wt-%

1. Schematic diagram of thermomechanical process with tempering treatments for strips Nb, Nb–Mo and Nb–3Mo

1. Schematic diagram of thermomechanical process with tempering treatments for strips Nb, Nb–Mo and Nb–3Mo

2. Scanning electron micrographs showing as received microstructures in a strip Nb, b strip Nb–Mo and c strip Nb–3Mo (R.D., rolling direction)

2. Scanning electron micrographs showing as received microstructures in a strip Nb, b strip Nb–Mo and c strip Nb–3Mo (R.D., rolling direction)

3. Typical TEM images showing a ferrite with interior strain induced Nb carbides and b granular bainite in strip Nb–3Mo

3. Typical TEM images showing a ferrite with interior strain induced Nb carbides and b granular bainite in strip Nb–3Mo

Table 2. Volume percentage of phases in three hot rolled strips*

4. a electron backscatter diffraction map of strip Nb, b gradient of misorientation from point A to B in purple region, c gradient of misorientation from point C to point D in green region and d, e corresponding simulated Kikuchi patterns at points A and B in a

4. a electron backscatter diffraction map of strip Nb, b gradient of misorientation from point A to B in purple region, c gradient of misorientation from point C to point D in green region and d, e corresponding simulated Kikuchi patterns at points A and B in a

5. Misorientation angle profiles for strips Nb, Nb-Mo and Nb-3Mo

5. Misorientation angle profiles for strips Nb, Nb-Mo and Nb-3Mo

Table 3. List of 24 axis angle pairs for adjacent grains A and B

6. a substructure of tempered granular bainite in strips Nb with tempering at 600°C for 1 h, b distribution of nanometre sized carbides located at given dislocation lines in enlarged region of a with dashed white frame, c Moiré fringes of nanometre sized carbides, indicated by arrows in enlarged region of b with dashed white frame and d corresponding FFT image of carbides and bainitic matrix in c

6. a substructure of tempered granular bainite in strips Nb with tempering at 600°C for 1 h, b distribution of nanometre sized carbides located at given dislocation lines in enlarged region of a with dashed white frame, c Moiré fringes of nanometre sized carbides, indicated by arrows in enlarged region of b with dashed white frame and d corresponding FFT image of carbides and bainitic matrix in c

Table 4. Dislocation density of granular bainite after tempering at 600°C for different time intervals

7. Hardness of granular bainite versus tempering time at a 650°C, b 600°C and c 550°C

7. Hardness of granular bainite versus tempering time at a 650°C, b 600°C and c 550°C

8. Images (HR-TEM) illustrating Moiré fringes of nanometre sized carbides at bainitic matrix in a strip Nb, c strip Nb–Mo and e strip Nb–3Mo and b, d, f corresponding FFT images for strips tempered at 600°C for 1 h

8. Images (HR-TEM) illustrating Moiré fringes of nanometre sized carbides at bainitic matrix in a strip Nb, c strip Nb–Mo and e strip Nb–3Mo and b, d, f corresponding FFT images for strips tempered at 600°C for 1 h

9. Energy dispersive X-ray spectrum of (NbxMo1−x) carbides precipitated at bainitic matrix, being individually examined at a strip Nb–Mo and b strip Nb–3Mo after tempering at 600°C for 1 h

9. Energy dispersive X-ray spectrum of (NbxMo1−x) carbides precipitated at bainitic matrix, being individually examined at a strip Nb–Mo and b strip Nb–3Mo after tempering at 600°C for 1 h

Table 5. Yield/tensile strength (MPa) of as rolled strips after tempering at 600°C for different time intervals

Table 6. Elongation (%) of as rolled strips after tempering at 600°C for different time intervals