Abstract
FeAl–TiC nanocomposite was successfully synthesised by the ball milling of Fe, Al, Ti and graphite powder mixture. The structural and morphological evolutions of the powders were studied by X-ray diffraction and scanning electron microscopy respectively. Results show that reactions forming of FeAl and TiC began after 6 h of milling and completed after 12 h of milling. The minimum mean grain size and maximum microstrain values of FeAl were 5·5 nm and 1·8% at the end of milling. Maximum microhardness value of the 12 h milled and annealed powder was 8·75 GPa. Scanning electron microscopy images and particle size measurement showed that very fine spheroid particles (3·4 μm) were prepared at the end of milling.
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