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Analytical Letters Volume 18, 1985 - Issue 4
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SEPARATIONS

Quantitative Separation of Pd(II) by TLC of Metal Ions on Cerium (IV) Antimonate

N. S. Seth Chemistry Department, Bareilly College, Bareilly, 243 001, INDIA
,
R. P. S. Rajput Chemistry Department, Bareilly College, Bareilly, 243 001, INDIA
,
N. K. Agrawal Chemistry Department, Bareilly College, Bareilly, 243 001, INDIA
,
Sunil K. Agrawal Chemistry Department, Bareilly College, Bareilly, 243 001, INDIA
&
Shachi Agrawal Chemistry Department, Bareilly College, Bareilly, 243 001, INDIA
Pages 481-486 | Received 01 Oct 1984, Accepted 05 Dec 1984, Published online: 05 Dec 2006
 
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Abstract

A quantitative TLC separation of metal ions using cerium (IV) antimonate as the solid phase are described. Using an acetonitrile- HNO3 solvent Pb2+ can be separated quantitatively (2–10 μg) from several other ions. A quantitative spectrophotometric assay using p-nitroso-dimethylaniline is proposed.

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