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Analytical Letters Volume 50, 2017 - Issue 9
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LIQUID CHROMATOGRAPHY

Determination of Meropenem and Ertapenem in Lagoon Water, Bedding Soil, and Silage by High-Performance Liquid Chromatography–Tandem Mass Spectrometry

Yuan LiuNational Reference Laboratory for Veterinary Drug Residues, College of Veterinary Medicine, China Agricultural University, Beijing, China
,
Jianye LiuNational Reference Laboratory for Veterinary Drug Residues, College of Veterinary Medicine, China Agricultural University, Beijing, China
,
Xiaowei LiNational Reference Laboratory for Veterinary Drug Residues, College of Veterinary Medicine, China Agricultural University, Beijing, China
,
Kunxia ZhaoNational Reference Laboratory for Veterinary Drug Residues, College of Veterinary Medicine, China Agricultural University, Beijing, China
,
Pengchun ZhangNational Reference Laboratory for Veterinary Drug Residues, College of Veterinary Medicine, China Agricultural University, Beijing, China
&
Shuangyang DingNational Reference Laboratory for Veterinary Drug Residues, College of Veterinary Medicine, China Agricultural University, Beijing, ChinaCorrespondence[email protected]
Pages 1387-1396 | Received 06 Jul 2016, Accepted 16 Aug 2016, Published online: 11 Jul 2017
 
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ABSTRACT

A simple and sensitive method was developed and validated by high-performance liquid chromatography–tandem mass spectrometry (HPLC–MS/MS) for the determination of meropenem and ertapenem in environmental materials from dairy farms. The limits of quantification were between 1 and 20 ng/mL for the analytes in lagoon water, bedding soil, and silage. The recoveries for meropenem and ertapenem exceeded 80%. The intraday and interday precision values were less than 15% in all samples. The validated method was employed to determine the meropenem and ertapenem in environment samples obtained from dairy farms.

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