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Ferroelectrics Volume 568, 2020 - Issue 1
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Study on milling time and calcining temperature of A-site-doped BNT-BLT anti-ferroelectric ceramics

Yongfeng WangSchool of Materials Science and Engineering, Xi’an Aeronautical University, Xi’an, P.R. ChinaCorrespondence[email protected]
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,
Jing CaoSchool of Materials Science and Engineering, Xi’an Aeronautical University, Xi’an, P.R. ChinaView further author information
&
Zhao LiSchool of Materials Science and Engineering, Xi’an Aeronautical University, Xi’an, P.R. ChinaView further author information
Pages 47-54 | Received 21 Aug 2019, Accepted 31 Mar 2020, Published online: 03 Nov 2020
 
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Abstract

[(Bi1/2Na1/2)0.94Ba0.06]0.97La0.02TiO3 (BNT-BLT) lead-free anti-ferroelectric ceramics were synthesized by a conventional solid-state.By analyzing TGA and DSC curves, the material should be calcined at about 800 °C. The effects of different milling time on the microstructure of the materials were also studied. Microstructures analysis and the calculation from the X-ray diffraction results reveal that the milling time of BNT-BLT ceramic should be controlled within a reasonable range, around 15 h.

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Funding

This work was supported by the Natural Science Foundation of Shanxi (2019217314GXRC009CG010-GXYD9.1)

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