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Ferroelectrics Volume 152, 1994 - Issue 1
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Original Articles

Pb(ZrxTi1-x)O3 films produced by sol-gel proceslng: Thin film growth and properties

R. Le Bihan Laboratoire de Physique des Surfaces, Université de Nantes 2, rue de la Houssiniè, e - 44072, Nantes, Cedex, 03, FRANCE
,
A. Micheiet Laboratoire de Physique des Surfaces, Université de Nantes 2, rue de la Houssiniè, e - 44072, Nantes, Cedex, 03, FRANCE
,
J. L. Charter Laboratoire de Physique des Surfaces, Université de Nantes 2, rue de la Houssiniè, e - 44072, Nantes, Cedex, 03, FRANCE
,
S. Ouvrard Laboratoire de Physique des Surfaces, Université de Nantes 2, rue de la Houssiniè, e - 44072, Nantes, Cedex, 03, FRANCE
&
Em. Hafid Laboratoire de Physique des Surfaces, Université de Nantes 2, rue de la Houssiniè, e - 44072, Nantes, Cedex, 03, FRANCE
Pages 13-18 | Received 09 Aug 1993, Published online: 25 Feb 2011
 
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Abstract

PZT thin films of various compositions have been grown by sol-gel processing. After firing and annealing at various temperatures and heating rates, the crystallinity is checked by X-ray diffraction, ferroelectricity by observation of hysteresis loop, stoichiometry by EMA and surface morphology by SEM. A study by XPS is undergone. Ferroelectric domains are present and visualized with TEM.

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