ABSTRACT
To improve the bonding strength of precision adhesive joints, mechanical and electrochemical surface treatments were combined to modify the original bonding surfaces. Microgrooves with different aspect ratios were manufactured on aluminum-alloy surfaces and phosphoric acid anodizing (PAA) was then applied to the surfaces. Wettability, shear strength, and fracture morphology were tested and analyzed. PAA treatment could change the original flat surface to be hydrophilic, and microgrooves could further enhance these characteristics. Compared with the original flat surface, the shear strength of the micro-structured surfaces without PAA treatment increased by 8.54% at an aspect ratio of 0.02, but decreased by 0.22% and 1.90% as the aspect ratio increased to 0.04 and 0.08, respectively. The shear strength of the flat surface only treated by PAA increased by 22.88%, while combining microgrooves could further improve the shear strength by 38.17%, 39.09%, and 42.24% at aspect ratios of 0.02, 0.04, and 0.08, respectively. Fracture morphology analysis and observation of interfacial wetting indicated that manufacturing microgrooves and applying PAA treatment on the aluminum-alloy surfaces could eliminate many tiny interface failures and greatly increase the effective bonding area, which significantly improved the shear strength.
Acknowledgments
The authors thank the support from the National Key Research and Development Program of China (No. 2022YFB3403801), the Foundation Enhancement Program (No. 2022-JCJQ-JJ-0102), the Major Fundamental Research of Equipment (514010208-301), the National Fundamental Scientific Research (No. JCKY2022203B006), the National Natural Science Foundation of China (No. 51935003), and the Project of Cultivation for young top-match Talents of Beijing Municipal Institutions (No. BPHR202203035).
Disclosure statement
No potential conflict of interest was reported by the author(s).