Copolymerization of N-Vinylcarbazole with 2-Dimethylaminoethyl Methacrylate

I. Sideridou-karayannidou Department of Chemistry, Aristotle University, GR-540 06, Thessaloniki, Greece

G. Karayannidis Department of Chemistry, Aristotle University, GR-540 06, Thessaloniki, Greece

P. Mavros Department of Chemistry, Aristotle University, GR-540 06, Thessaloniki, Greece

K. A. Tsoleridis Department of Chemistry, Aristotle University, GR-540 06, Thessaloniki, Greece

M. Tzitzidou Department of Chemistry, Aristotle University, GR-540 06, Thessaloniki, Greece

Abstract

The thermal copolymerization of N-vinylcarbazole (VCz) with 2-dimethylaminoethyl methacrylate (DMAEM) initiated by α,α′-azobisisobutyronitrile (AIBN) in solution in tetrahydrofuran at 60°C has been studied. Different compositions of copolymer were prepared and characterized by UV, IR, and ¹H-NMR spectroscopy, viscosity measurements, and thermal studies. The estimation of the composition of VCz and DMAEM in the copolymer was carried out by UV spectroscopy. The reactivity ratio of VCz (r ₁) and DMAEM (r ₂) was determined by the methods of Mayo and Lewis, Kelen and Tüdös, and Tidwell and Mortimer.

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Copolymerization of N-Vinylcarbazole with 2-Dimethylaminoethyl Methacrylate

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Copolymerization of N-Vinylcarbazole with 2-Dimethylaminoethyl Methacrylate

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