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Molecular Physics
An International Journal at the Interface Between Chemistry and Physics
Volume 117, 2019 - Issue 19: 15th International Symposium on Spin and Magnetic Field Effects in Chemistry and Related Phenomena (SCM 2017)
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Spin Chemistry Meeting 2017

Same spectral signature in liquid-state and solid-state 1H photo-CIDNP NMR spectra of cyclohexanone

Mikhail PanovInternational Tomography Center, Siberian Branch of Russian Academy of Science, Novosibirsk, Russia;Novosibirsk State University, Novosibirsk, RussiaView further author information
,
Pavlo BielytskyiUniversität Leipzig, Institut für Analytische Chemie, Leipzig, GermanyView further author information
,
Daniel GräsingUniversität Leipzig, Institut für Analytische Chemie, Leipzig, GermanyView further author information
,
Alexandra YurkovskayaInternational Tomography Center, Siberian Branch of Russian Academy of Science, Novosibirsk, Russia;Novosibirsk State University, Novosibirsk, RussiaCorrespondence[email protected]
View further author information
&
Jörg MatysikUniversität Leipzig, Institut für Analytische Chemie, Leipzig, GermanyCorrespondence[email protected]
ORCID Iconhttps://orcid.org/0000-0002-7800-7443View further author information
ORCID Icon
Pages 2756-2761 | Received 30 Apr 2018, Accepted 30 Jul 2018, Published online: 26 Aug 2018
 
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ABSTRACT

For the first time, a 1H solid-state photo-CIDNP effect is reported. The effect is observed in frozen solution of cyclohexanone in 1,4-dioxane-d8 under magic-angle spinning and continuous irradiation by the full spectrum of a xenon arc lamp. The spectral features show close similarity with those observed by 1H liquid-state photo-CIDNP NMR.

GRAPHICAL ABSTRACT

Disclosure statement

No potential conflict of interest was reported by the authors.

Additional information

Funding

This work was supported by the Russian Science Foundation under grant 15-13-20035.

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