Simple and Efficient Method for the Synthesis of Azides in Water-THF Solvent System

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Acknowledgement

Authors M. S. and P. V. R. acknowledge the Principal, N. S. B. College, Nanded and the Director, Central Facility Building for Research and Development, Osmania University, Hyderabad for providing spectral facilities.

Notes

^aPurity based on GC analysis: column OV-1carrier gas flow H₂/N₂:18 mL/min. sample size 0.2 mL.

^bPurity by GC after distillation.

^cPurity based on GC-MS analysis: Isolated compound subjected to GC-MS by dissolving in DCM.

^dMelting point.