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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 35, 2005 - Issue 18
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Original Articles

Synthesis of Thiourea‐Bridged Cluster Glycoside Calixarenes

Yun Ge College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou, China
,
Yahua Cai College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou, China
&
Chaoguo Yan College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou, ChinaCorrespondence[email protected]
Pages 2355-2361 | Received 28 Feb 2005, Published online: 18 Aug 2006
 
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Abstract

Thiourea‐bridged peracetylated glycoside calixarenes have been smoothly synthesized by the addition reactions of tetraacetylglycosyl isothiocyanates with amidoamine derivatives of calix[4]resorcinarene and p‐tert‐butylcalix[n]arenas (n=6, 8) in high yields (40–75%). All the glycoside‐containing calixarenes were characterized by 1H NMR, IR spectroscopy, and elemental analysis.

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