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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 2
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Original Articles

DMSO/NaNO2/49% HBr: A Novel and Powerful Oxidant for the Direct Conversion of Primary Benzylamines to Benzoic Acids

Ramesh Naik Department of Studies in Chemistry, Central College Campus, Bangalore University, Bangalore, India
&
M. A. Pasha Department of Studies in Chemistry, Central College Campus, Bangalore University, Bangalore, IndiaCorrespondence[email protected]
Pages 165-168 | Received 14 Jul 2005, Published online: 15 Aug 2006
 
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Abstract

A mixture of DMSO, NaNO2, and 49% HBr is found to oxidize primary benzyl amines to benzoic acids at 100°C.

Acknowledgment

Ramesh Naik acknowledges the Bangalore University and State Bank of Mysore, Yidagur branch, for financial assistance and the Department of Organic Chemistry, Indian Institute of Science, Bangalore, for recording NMR spectra.

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