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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 2
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Original Articles

Facile Preparation and Purification of Mono tert‐Butyl Malonate

Vitali I. Tararov Leibniz‐Institut für Organische Katalyse e.V., Rostock, Germany
,
Andrei Korostylev Leibniz‐Institut für Organische Katalyse e.V., Rostock, Germany
,
Gerd König Ratiopharm GmbH, Ulm, Germany
&
Armin Börner Leibniz‐Institut für Organische Katalyse e.V., Rostock, Germany; Institut für Chemie der Universität Rostock, Rostock, GermanyCorrespondence[email protected]
Pages 187-191 | Received 14 Jun 2005, Published online: 15 Aug 2006
 
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Abstract

Reaction of Meldrum's acid with tert‐BuOH gives tert‐BuO2CCH2CO2H, which can be easily purified via its corresponding crystalline ammonium salt and subsequent acidification.

Acknowledgment

We thank K. Mevius for skilled technical assistance. Financial support from Ratiopharm GmbH is gratefully acknowledged.

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