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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 15
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Original Articles

Rapid Microwave‐Promoted Catalyst‐ and Solvent‐Free Suzuki‐Type Coupling Reaction

Jie Yan College of Chemical Engineering and Materials Sciences, Zhejiang University of Technology, Hangzhou, Zhejiang, ChinaCorrespondence[email protected]
,
Weixiao Hu College of Pharmaceutical Sciences, Zhejiang University of Technology, Hangzhou, Zhejiang, China
&
Wei Zhou College of Pharmaceutical Sciences, Zhejiang University of Technology, Hangzhou, Zhejiang, China
Pages 2097-2102 | Received 12 Dec 2005, Published online: 16 Feb 2007
 
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Abstract

The catalyst‐ and solvent‐free Suzuki coupling reaction of sodium tetraphenylborate with hypervalent iodonium salts was achieved under microwave irradiation in the absence of a base. A convenient method for formation of carbon–carbon bonds afforded good yields in a short time.

Acknowledgment

Financial support from the Zhejiang Province Natural Science Foundation of China (Project Y404016) and Zhejiang Province Education Foundation of China (Project 20040569) is greatly appreciated.

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