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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 15
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Original Articles

P2O5/SiO2‐Catalyzed One‐Pot Synthesis of Amides from Ketones via Schmidt Reaction under Microwave Irradiation in Dry Media

Hossein Eshghi Department of Chemistry, Ferdowsi University of Mashhad, Mashhad, Iran; Department of Chemistry, Sistan and Baluchestan University, Zahedan, IranCorrespondence[email protected]
&
Asadollah Hassankhani Department of Chemistry, Sistan and Baluchestan University, Zahedan, Iran
Pages 2211-2216 | Received 16 Aug 2005, Published online: 16 Feb 2007
 
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Abstract

A facile and efficient method for the preparation of amides from ketones by the Schmidt reaction is described for the first time using P2O5/SiO2 and sodium azide under solvent‐free microwave irradiation. Advantages of this procedure are selectivity, good yields, a simple operation, short reaction time, and solvent‐free conditions.

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