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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 15
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Original Articles

Simple Method for the Preparation of Dimethyl Acetals from Ketones with Montmorillonite K 10 and p‐Toluenesulfonic Acid

Horacio Mansilla Instituto de Productos Naturales y Agrobiología del C.S.I.C., La Laguna, Tenerife, SpainCorrespondence[email protected]
&
David Regás Instituto Universitario de Bioorgánica “Antonio González,”, Universidad de la Laguna, La Laguna, Tenerife, Spain
Pages 2195-2201 | Received 24 Oct 2005, Published online: 16 Feb 2007
 
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Abstract

A simple method for conversion of ketones to their corresponding dimethyl acetals using montmorillonite K 10 and p‐toluenesulfonic acid as acidic cocatalysts under very mild reaction conditions is described.

Acknowledgments

This research was made possible by grant BQU2001‐3184 from the Spanish Ministry of Science and Technology. D. R. thanks CajaCanarias for a SEGAI fellowship.

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