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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 16
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Original Articles

Alumina–Methanesulfonic Acid (AMA)/NaNO2 as an Efficient Procedure for the Chemoselectivite N‐Nitrosation of Secondary Amines

Khodabakhsh Niknam Department of Chemistry, Faculty of Sciences, Persian Gulf University, Bushehr, IranCorrespondence[email protected]
&
Mohammad Ali Zolfigol Department of Chemistry, College of Science, Bu‐Ali Sina University, Hamadan, Iran
Pages 2311-2319 | Published online: 22 Sep 2006
 
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Abstract

A combination of alumina/methanesulfonic acid (AMA) and sodium nitrite was used as an effective nitrosating agent for the nitrosation of secondary amines under mild and heterogeneous conditions in good to excellent yields.

Acknowledgment

We are thankful to the Persian Gulf University Research Council for partial support of this work.

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