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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 24
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Original Articles

Facile Deprotection of 1,3‐Oxathiolanes to Carbonyl Compounds with O‐Iodoxy Benzoic Acid (IBX) in the Presence of β‐Cyclodextrin in WaterFootnote

M. Somi Reddy Organic Chemistry Division I, Indian Institute of Chemical Technology, Hyderabad, India
,
M. Narender Organic Chemistry Division I, Indian Institute of Chemical Technology, Hyderabad, India
,
A. Mahesh Organic Chemistry Division I, Indian Institute of Chemical Technology, Hyderabad, India
,
Y. V. D. Nageswar Organic Chemistry Division I, Indian Institute of Chemical Technology, Hyderabad, India
&
K. Rama Rao Organic Chemistry Division I, Indian Institute of Chemical Technology, Hyderabad, IndiaCorrespondence[email protected]
Pages 3771-3775 | Received 05 May 2006, Published online: 01 Dec 2006
 
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Abstract

1,3‐Oxathiolanes are smoothly deprotected to carbonyl compounds by IBX at room temperature with β‐cyclodextrin as a catalyst and water as solvent.

IICT Communication No. 060424.

Acknowledgment

M. S. R., M. N. and A. M. thank to CSIR, New Delhi, India, for financial assistance.

Notes

IICT Communication No. 060424.

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