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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 5
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Original Articles

Microwave‐Promoted, Solvent‐Free, Three‐Component Coupling of Aldehyde, Alkyne, and Amine Catalyzed by AgNO3

Tingting He Hefei National Laboratory for Physical Science at Microscale and Department of Chemistry, University of Science and Technology of China, Hefei, China
,
Zhenggen Zha Hefei National Laboratory for Physical Science at Microscale and Department of Chemistry, University of Science and Technology of China, Hefei, China
,
Chongfeng Pan Hefei National Laboratory for Physical Science at Microscale and Department of Chemistry, University of Science and Technology of China, Hefei, China
&
Zhiyong Wang Hefei National Laboratory for Physical Science at Microscale and Department of Chemistry, University of Science and Technology of China, Hefei, ChinaCorrespondence[email protected]
Pages 849-858 | Published online: 10 Mar 2007
 
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Abstract

An efficient three‐component coupling reaction of alkyne, aldehyde, and amine was carried out in one pot smoothly under the catalysis of AgNO3 and microwave irradiation. The scope of reaction substrates was extended. Moreover, the reaction can be performed under solvent‐free condition, affording propargylamine derivatives with high yields.

Acknowledgment

The authors are grateful to National Nature Science Foundation of China (Nos. 20472078 and 30572234) for their support.

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