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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 6
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Original Articles

PEG‐Supported Sulfonic Acid as an Efficient and Recyclable Catalyst for the Synthesis of 1,1‐Diacetates under Solvent‐Free Conditions

Qiu‐Ying Wang College of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang, China
,
Shou‐Ri Sheng College of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang, ChinaCorrespondence[email protected]
,
Mei‐Hong Wei College of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang, China
,
Zhong‐Li Xie College of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang, China
&
Xiao‐Ling Liu College of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang, China
Pages 1019-1026 | Received 26 Jun 2006, Published online: 24 Feb 2007
 
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Abstract

An operationally simple, efficient, and environmentally benign synthesis of 1,1‐diacetates in good yields by reaction of different aldehydes with acetic anhydride in the presence of PEG‐supported sulfonic acid under solvent‐free conditions is described.

Acknowledgment

We gratefully acknowledge financial support from the National Natural Science Foundation (NSF) of China (No. 20562005) and NSF of Jiangxi Province (No. 0620021).

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