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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 10
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Original Articles

Fast and Efficient Synthesis of 10‐Aryl‐2,7‐dimethyl‐4,5‐dioxo‐3,6,9‐trioxa‐3,4,5,6,9,10‐hexahydroanthracene under Microwave Irradiation without Catalyst

Yuan Gao Department of Chemistry, Shenzhen University, Guangdong, Shenzhen, China
,
Shujiang Tu Department of Chemistry, Xuzhou Normal University, Jiangsu, Xuzhou, ChinaCorrespondence[email protected]
,
Feng Shi Department of Chemistry, Xuzhou Normal University, Jiangsu, Xuzhou, China
,
Qian Wang Department of Chemistry, Xuzhou Normal University, Jiangsu, Xuzhou, China
,
Xiaotong Zhu Department of Chemistry, Xuzhou Normal University, Jiangsu, Xuzhou, China
&
Daqing Shi Department of Chemistry, Xuzhou Normal University, Jiangsu, Xuzhou, China
Pages 1603-1608 | Received 12 Apr 2006, Published online: 22 May 2007
 
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Abstract

A fast and efficient synthetic method for the title compounds is described. By heating aromatic aldehyde and triacetic acid lactone in ethylene glycol under microwave irradiation without catalyst for 3–5 min, 10‐aryl‐2,7‐dimethyl‐4,5‐dioxo‐3,6,9‐trioxa‐3,4,5,6,9,10‐hexahydroanthracenes were afforded with high yields.

Acknowledgment

We thank the Natural Science Foundation of Guangdong Province (No. 031792) for financial support.

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