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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 16
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Original Articles

Synthesis of Novel Greener Functionalized Ionic Liquids Containing Appended Hydroxyl

Guo Ren Feng Key Laboratory of Organosilicon Chemistry and Material Technology of Ministry of Education, Hangzhou Teachers College, Hangzhou, China
,
Jia Jian Peng Key Laboratory of Organosilicon Chemistry and Material Technology of Ministry of Education, Hangzhou Teachers College, Hangzhou, China
,
Hua Yu Qiu Key Laboratory of Organosilicon Chemistry and Material Technology of Ministry of Education, Hangzhou Teachers College, Hangzhou, China
,
Jian Xiong Jiang Key Laboratory of Organosilicon Chemistry and Material Technology of Ministry of Education, Hangzhou Teachers College, Hangzhou, China
,
Lan Tao Key Laboratory of Organosilicon Chemistry and Material Technology of Ministry of Education, Hangzhou Teachers College, Hangzhou, ChinaCorrespondence[email protected]
&
Guo Qiao Lai Key Laboratory of Organosilicon Chemistry and Material Technology of Ministry of Education, Hangzhou Teachers College, Hangzhou, China
Pages 2671-2675 | Received 27 Dec 2006, Published online: 14 Aug 2007
 
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Abstract

Novel “greener” functionalized ionic liquids have been prepared by the reaction of 1,2‐epoxy propane and dilute sulfuric acid with [EMIm]Br or [BMIm]Br formed by alkyl bromide (RBr) and 1‐methylimidazole. This kind of ionic liquid could be possibly used as green solvent and catalyst, especially as phase‐transfer catalyst in organic chemistry (e.g., the synthesis of ethoxybenzene). Their chemical structures were characterized by 1H NMR, 13C NMR, and IR.

Acknowledgments

We are grateful to Hangzhou Teachers College Science Foundation (2006 XNZ08) for financial support.

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