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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 20
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Original Articles

Novel Synthesis and Characterization of 1,3‐Bis(2‐dihydrothiazolyl)thiaalkoxy‐ptert‐butylcalix[4]arenes

, &
Pages 3479-3484 | Received 09 Feb 2007, Published online: 05 Oct 2007
 

Abstract

A novel series of 1,3‐bis(2‐dihydrothiazolyl)thiaalkoxy‐ptert‐butylcalix[4]arenes generated by the reaction between 4,5‐dihydrothiazole‐2‐thiol and the different dibromide calix[4]aryl groups have been synthesized and structurally characterized by IR, 1H NMR, 13C NMR, and MS. From their analytical data, it was found that compounds 8, 9, and 10 had cone conformations, whereas compound 11 existed as a mixture conformation. To verify the structure of the synthetic compounds, a single‐crystal X‐ray structure of compound 8 was obtained.

Acknowledgments

Thanks for the support of the National Natural Science Foundation of China (No. 20376059).

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