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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 21
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Original Articles

Samarium Triiodide–Catalyzed Formation of Mannich‐Type Products by Amidoalkylation of 1,3‐Dicarbonyl Compounds

Xiaoxia Wang Zhejiang Key Laboratory for Reactive Chemistry on Solid Surfaces, College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua, China E-mail: [email protected]Correspondence[email protected]
,
Hui Mao Zhejiang Key Laboratory for Reactive Chemistry on Solid Surfaces, College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua, China E-mail: [email protected]
,
Yan Yu Zhejiang Key Laboratory for Reactive Chemistry on Solid Surfaces, College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua, China E-mail: [email protected]
,
Xiudan Zhu Zhejiang Key Laboratory for Reactive Chemistry on Solid Surfaces, College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua, China E-mail: [email protected]
&
Chunlan Zhu Zhejiang Key Laboratory for Reactive Chemistry on Solid Surfaces, College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua, China E-mail: [email protected]
Pages 3751-3758 | Received 13 Apr 2007, Published online: 19 Oct 2007
 
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Abstract

With samarium triiodide (SmI3) as a catalyst, the amidoalkylation of 1,3‐dicarbonyl compounds with N‐(1‐benzotriazol‐1‐ylalkyl)amides proceeded readily under mild conditions to afford Mannich‐type products in good to excellent yields.

Acknowledgments

We are grateful to the Natural Science Foundation of Zhejiang Province (Project No. Y405035) for financial support.

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