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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 38, 2008 - Issue 2
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Original Articles

Unexpectedly High Activity of Zn(OTf)2 · 6H2O in Catalytic Friedel–Crafts Acylation Reaction

Fei He College of Chemistry and Materials Science, Wenzhou University, Wenzhou, China
,
Huayue Wu College of Chemistry and Materials Science, Wenzhou University, Wenzhou, China
,
Jiuxi Chen College of Chemistry and Materials Science, Wenzhou University, Wenzhou, China
&
Weike Su College of Chemistry and Materials Science, Wenzhou University, Wenzhou, China; College of Pharmaceutical Sciences, Zhejiang University of Technology, Zhejiang Key Laboratory of Pharmaceutical Engineering, Hangzhou, ChinaCorrespondence[email protected]
Pages 255-264 | Received 18 Mar 2007, Published online: 18 Jan 2008
 
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Abstract

Zn(OTf)2 · 6H2O was used to promote Friedel–Crafts acylation of aromatics. The work describes the high activity and efficiency of Zn(OTf)2 · 6H2O in acylation of aromatics, and the catalyst has surpassed most metal triflates in dispensing when dried at high temperature under vacuum before use.

Acknowledgment

We are grateful to the National Natural Science Foundation of China (Grant Nos. 20476098 and 20676123) for financial support.

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