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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 38, 2008 - Issue 7
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Original Articles

Solvent‐Free Passerini Reactions

Dominik Koszelewski Institute of Organic Chemistry, Polish Academy of Sciences, Kasprzaka 44/52, 01‐224, Warsaw, Poland
,
Wiktor Szymanski Institute of Organic Chemistry, Polish Academy of Sciences, Kasprzaka 44/52, 01‐224, Warsaw, Poland
,
Joanna Krysiak Institute of Organic Chemistry, Polish Academy of Sciences, Kasprzaka 44/52, 01‐224, Warsaw, Poland
&
Ryszard Ostaszewski Institute of Organic Chemistry, Polish Academy of Sciences, Kasprzaka 44/52, 01‐224, Warsaw, PolandCorrespondence[email protected]
Pages 1120-1127 | Received 30 May 2007, Published online: 12 Mar 2008
 
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Abstract

The influence of the substrate structure and concentration on the yield of the Passerini reaction was studied. A new, solvent‐free methodology for a convenient preparation of α‐acyloxyamides 4 was established and compared to the classical methodology. A higher reaction yield was obtained in shorter time, especially in the case of aromatic aldehydes.

Acknowledgment

This work was supported by the grants from the Polish State Committee for Scientific Research, No. PBZ‐KBN‐126/T09/07, PBZ‐MIN‐007/P04/2003.

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