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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 38, 2008 - Issue 10
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Original Articles

Catalytic Transfer Hydrogenation and Hydrogenolysis in Ionic Liquids with Pd/MgLa Mixed Oxide and Pd/MgAl Hydrotalcite as Recyclable Catalysts

Zoltán Baán Department of Organic Chemical Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Attila Potor Department of Organic Chemical Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Agnieszka Cwik Department of Organic Chemical Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Zoltán Hell Department of Organic Chemical Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
György Keglevich Department of Organic Chemical Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Zoltán Finta Chinoin Pharmaceutical and Chemical Works Ltd., Budapest, Hungary
&
István Hermecz Chinoin Pharmaceutical and Chemical Works Ltd., Budapest, HungaryCorrespondence[email protected]
 show all
Pages 1601-1609 | Received 25 Oct 2007, Published online: 24 Apr 2008
 
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Abstract

A new Pd/MgLa mixed oxide and the known Pd/MgAl hydrotalcite catalysts were applied and recycled successfully in catalytic transfer hydrogenation reactions in ionic liquids. Some α,β‐unsaturated carboxylic acid derivatives were hydrogenated in excellent yields. The catalysts were recycled without significant loss of activity. Besides that, a number of halogenated aromatic compounds were dehalogenated under similar catalytic transfer conditions.

Acknowledgment

Z.B. is grateful for a PhD fellowship from Sanofi‐Aventis (Chinoin) and the Varga József Foundation.

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