Abstract
A quick, efficient, one-pot synthesis of dithiocarbazates was accomplished in high yields by the reaction of various tosylates of primary, secondary, and tertiary alcohols with a variety of substituted hydrazines using the benzyl–trimethylammonium hydroxide (Triton-B)/CS2 system. The reaction conditions are mild with simpler workup procedures than the reported methods.
ACKNOWLEDGMENTS
Authors thank the Sophisticated Analytical Instrument Facility (SIAF) division of Central Drug Research Institute (CDRI) for providing spectroscopic and analytical data.
Notes
Note. All the products were characterized by IR, NMR, and mass spectroscopic data.