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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 39, 2009 - Issue 17
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Original Articles

Unexpected Reaction of Oximinoacetoacetate with Amines: A Novel Synthesis of Carbamates

Ibrahim Elghamry Institute of Organic and Biomolecular Chemistry, Georg-August-University Göttingen, Göttingen, GermanyCorrespondence[email protected]
Pages 3010-3015 | Received 06 Oct 2008, Published online: 03 Aug 2009
 
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Abstract

The synthesis of alkyl carbamates by a solvent-free reaction of oximinoacetoacetate and amine at 130°C is reported. A preliminary mechanism to this unexpected reaction is also given.

ACKNOWLEDGMENT

The author thanks the Alexander von Humboldt Foundation for the research fellowship (Long-Term Co-operation Program) at the Georg-August-University in Göttingen, Germany.

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