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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 39, 2009 - Issue 13
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Original Articles

Solvent- and Catalyst-Free Synthesis of New Unsymmetrical Multidentate Thio-bis-aminophenol Ligands by Mannich Condensation

Abbas Shockravi Faculty of Chemistry, Tarbiat Moallem University, Tehran, IranCorrespondence[email protected]
,
Mahdieh Sadeghpour Faculty of Chemistry, Tarbiat Moallem University, Tehran, Iran; Department of Chemistry, Islamic Azad University, Takestan Branch, Qazvin, Iran
&
Abolfazl Olyaei Department of Chemistry, Payame Noor University, Qazvin, Iran
Pages 2347-2359 | Received 13 Sep 2008, Published online: 01 Jun 2009
 
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Abstract

A one-pot, three-component, Mannich condensation of electron-rich aromatic compounds such as 5-methyl-2-hydroxyphenyl sulfide, 2-aminopyrimidine, and various aromatic aldehydes were used to prepare a series of new unsymmetrical multidentate aminophenol ligands. These compounds were synthesized in solvent-free conditions as a fast, simple, convenient, and uncatalyzed method. Details of the reaction conditions are discussed.

ACKNOWLEDGMENT

We thank the Research Council of the Tarbiat Moallem University for financial support.

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