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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 39, 2009 - Issue 19
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Original Articles

Green Route for Rapid Synthesis of 2,2′-Dithiobis(benzothiazole) by Microwave Irradiation

Xin Wang Department of Chemistry, College of Basic Medicine, Anhui Medical University, Hefei, Anhui, China
,
Xianliang Chen Department of Chemistry, College of Basic Medicine, Anhui Medical University, Hefei, Anhui, China
,
Xiaojing Wu School of Chemical Engineering, Hefei University of Technology, Hefei, Anhui, ChinaCorrespondence[email protected]
,
Jingqiu Tao First Clinical College, Anhui Medical University, Hefei, Anhui, China
&
Ling Cheng School of Chemical Engineering, Hefei University of Technology, Hefei, Anhui, China
Pages 3453-3458 | Received 06 Oct 2008, Published online: 04 Sep 2009
 
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Abstract

A green route for rapid synthesis of 2,2′-dithiobis(benzothiazole) (DM) by microwave irradiation is discussed. The reaction time was shortened to 5 min, and the yield of product was good.

ACKNOWLEDGMENT

This project was supported by Anhui Medical University.

Notes

Note. M 0.835 g, hydrogen peroxide 0.7 ml, irradiation time 5 min.

Note. M 0.835 g, irradiation time 5 min, 400 W.

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