Abstract
A green route for rapid synthesis of 2,2′-dithiobis(benzothiazole) (DM) by microwave irradiation is discussed. The reaction time was shortened to 5 min, and the yield of product was good.
ACKNOWLEDGMENT
This project was supported by Anhui Medical University.
Notes
Note. M 0.835 g, hydrogen peroxide 0.7 ml, irradiation time 5 min.
Note. M 0.835 g, irradiation time 5 min, 400 W.