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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 40, 2010 - Issue 4
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Original Articles

Green, Microwave-Assisted Approach to the Synthesis of Arylidene-Substituted Spiro[4,5]decan-8-one Derivatives in Water

Ju-Hua Peng Lianyungang Teachers' College, Lianyungang, Jiangsu, China
,
Xiao-Hong Zhang School of Chemistry and Chemical Engineering, Xuzhou Normal University, Xuzhou, Jiangsu, China
,
Feng Shi School of Chemistry and Chemical Engineering, Xuzhou Normal University, Xuzhou, Jiangsu, China
,
Wen-Juan Hao School of Chemistry and Chemical Engineering, Xuzhou Normal University, Xuzhou, Jiangsu, China
&
Shu-Jiang Tu Lianyungang Teachers' College, Lianyungang, Jiangsu, ChinaCorrespondence[email protected]
Pages 615-623 | Received 25 Mar 2009, Published online: 03 Feb 2010
 
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Abstract

A green approach to the synthesis of arylidene-substituted spiro[4,5]decan-8-one derivatives was successfully realized via the mild, base-catalyzed reaction of aromatic aldehydes with 1,4-dioxa-spiro[4.5]decan-8-one in water under microwave irradiation. This protocol has the prominent advantages of environmental friendliness, short reaction time, excellent yields, low cost, easy operation, and broad scope of applicability.

ACKNOWLEDGMENTS

We thank the National Natural Science Foundation of China (Nos. 20672090 and 200810102050) and the Key Item program of the Natural Science Foundation of Xuzhou Normal University (No. 07XLA04) for financial support.

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