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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 40, 2010 - Issue 9
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Original Articles

Convenient, Solvent-Free Method for Preparation of [Hydroxy(phosphoryloxy)iodo]arenes

Min Zhu College of Biological and Environmental Sciences, Zhejiang Shuren University, Hangzhou, ChinaCorrespondence[email protected]
,
Cheng Gang Cai College of Biological and Environmental Sciences, Zhejiang Shuren University, Hangzhou, China
,
Wei Ke College of Biological and Environmental Sciences, Zhejiang Shuren University, Hangzhou, China
&
Jing Shao College of Biological and Environmental Sciences, Zhejiang Shuren University, Hangzhou, China
Pages 1371-1376 | Received 12 Mar 2009, Published online: 07 Apr 2010
 
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Abstract

A convenient, solvent-free method for preparation of [hydroxy(phosphoryloxy)iodo]arenes is reported. (Diacetoxyiodo)benzene or other hypervalent iodine reagents and phosphates are simply blended and ground for several minutes in an agate mortar, giving good yields of [hydroxy(phosphoryloxy)iodo]arenes with excellent purities.

ACKNOWLEDGMENT

Financial support from the National Science Foundation of China (Project 20672100) is greatly appreciated.

Notes

a Isolated yield.

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