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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 40, 2010 - Issue 20
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Original Articles

New Deoxygenation Method for Amine N-Oxides Using Dimethylthiocarbamoyl Chloride

Hafize Caliskan Department of Chemistry, Trakya University, Edirne, TurkeyCorrespondence[email protected]
&
Ömer Zaim Department of Chemistry, Trakya University, Edirne, Turkey
Pages 3078-3083 | Received 04 May 2009, Published online: 13 Sep 2010
 
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Abstract

A facile and efficient deoxygenation method for various amine N-oxides to their corresponding amines is described. The experimental procedure is quite simple and the products are obtained in excellent yields.

ACKNOWLEDGMENT

We gratefully acknowledge the financial support of the Scientific Research Project Commission of Trakya University.

Notes

a Isolated yields.

b Reflux in (C2H5)3N.

c 3 eq. NaI used.

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