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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 40, 2010 - Issue 22
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Original Articles

Synthesis and Characterization of Six New Carbazolyl Porphyrins

, , , &
Pages 3315-3321 | Received 13 Apr 2009, Published online: 15 Oct 2010
 

Abstract

Novel 4-(N-carbazole methyl) benzoic acid and N-carbazolacetic acid are synthesized, then six new carbazolyl porphyrins are synthesized by bonding these acids to hydroxy porphyrin or amido porphyrin via acyl chloride or N,N′-dicyclohexylcarbodiimide (DCC)–dimethylaminopyndine methods. The formations of these title compounds, as well as their intermediates are characterized by 1H NMR, mass spectrometry, Fourier transform–infrared, and elemental analysis.

ACKNOWLEDGMENTS

The authors are grateful for the financial support of the National Natural Science Talent Foundation of China (No. J0830415), the Natural Science Foundation of Hunan Province (No. 05JJ30020), and the Development Foundation of the Scientific and Technological Bureau of Hunan Province (No. 04GK3035). We thank Dr. William Hickey for English editing.

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