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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 40, 2010 - Issue 23
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Original Articles

Convenient Route to Thiocarbonates from Alcohols, Thiols, and Triphosgene

Barahman Movassagh Department of Chemistry, K. N. Toosi University of Technology, Tehran, IranCorrespondence[email protected]
&
Mohammad Soleiman-Beigi Department of Chemistry, K. N. Toosi University of Technology, Tehran, Iran; Department of Chemistry, Ilam University, Ilam, Iran
Pages 3467-3471 | Received 03 Jun 2009, Published online: 05 Nov 2010
 
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Abstract

An efficient and simple one-pot, three-component procedure has been introduced for the preparation of various thiocarbonates from thiols, alcohols, and triphosgene in dichloromethane.

ACKNOWLEDGMENT

This work was supported by the K. N. Toosi University of Technology Research Council and the Iranian National Science Foundation (INSF, Grant No. 86063/21).

Notes

a Yields refer to those of pure isolated products characterized by IR, 1H NMR, and 13C NMR spectroscopy.

b References for known compounds.

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