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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 40, 2010 - Issue 3
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Original Articles

Microwave-Assisted Conjugate Addition of Pyrrole on Electron-Deficient Nitro-Olefins

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Pages 320-327 | Received 26 Aug 2008, Published online: 06 Jan 2010
 

Abstract

Michael addition of pyrrole to β-nitrovinyl compounds were carried out using microwave methodology. Monosubstituted pyrroles were obtained selectively in a major amount. Formation of novel product obtained during one of the reactions was explained by the double addition to nitrostyrene.

ACKNOWLEDGMENTS

We are grateful to Prof. M. S. Wadia for helpful discussions, Mr. A. P. Gadgil for IR spectra and elemental analysis, Mrs. J. P. Chaudhari for NMR spectra, and Mr. Shishupal for GC-MS.

Notes

a Yield calculated according to the recovered starting material.

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